Hit 1

FA	IDE(1); FLST(13); XREF(3); INP(6); CDER(2); MP(9); CRYPH(2); NMR(1); IR(1); UV(2); MS(1); POT(1); FINFO(2); RX(4); CNR(20)

Substance (1 of 1)

Beilstein Registry Number	90739
Beilstein Preferred RN	94-62-2
CAS Registry Number	94-62-2; 495-91-0; 7780-20-3; 30511-76-3; 30511-77-4
Chemical Name	1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidine; 1-Piperinoyl-piperidin; piperine
Autoname	5-benzo[1,3]dioxol-5-yl-1-piperidin-1-yl-penta-2,4-dien-1-one
Molecular Formula	C17H19NO3
Molecular Weight	285.34
Lawson Number	24081; 22876
Compound Type	heterocyclic
Constitution ID	38159
Tautomer ID	14686
Beilstein Reference	5-20-03-00469; 6-20
Entry Date	1988/06/27
Update Date	1994/01/18

Reference (1 of 20)

Citation Number	119906
Document Type	Journal
Authors	Stoklosa,K.
CODEN	BSCFAS
Journal Title	Bull.Soc.Chim.Fr.
Language Code	FR
Publication Year	1969
Page	3802-3806

Reference (2 of 20)

Citation Number	2605306
Document Type	Journal
Authors	Lloyd et al.
CODEN	JACSAT
Journal Title	J.Amer.Chem.Soc.
(Series) Volume	82
Publication Year	1960
Page	3791

Reference (3 of 20)

Citation Number	2835455
Document Type	Journal
Authors	Gupta et al.
CODEN	PYTCAS
Journal Title	Phytochemistry
(Series) Volume	11
Publication Year	1972
Page	2646

Reference (4 of 20)

Citation Number	3133321
Document Type	Journal
Authors	Dutta et al.
CODEN	IJSBDB
Journal Title	Indian J.Chem.Sect.B
(Series) Volume	15
Publication Year	1977
Page	583

Reference (5 of 20)

Citation Number	3133481
Document Type	Journal
Authors	Lurik et al.
CODEN	JGCHA4; ZOKHA4
Journal Title	J.Gen.Chem.USSR (Engl.Transl.); Zh.Obshch.Khim.
(Series) Volume	45; 45
Publication Year	1975; 1975
Page	2246; 2287

Reference (6 of 20)

Citation Number	3141536
Document Type	Journal
Authors	Mazeau; Zarzycki
CODEN	CHDCAQ
Journal Title	C.R.Hebd.Seances Acad.Sci.Ser.C
(Series) Volume	281
Publication Year	1975
Page	583,584

Reference (7 of 20)

Citation Number	3141959
Document Type	Journal
Authors	Loder et al.
CODEN	AJCHAS
Journal Title	Aust.J.Chem.
(Series) Volume	22
Publication Year	1969
Page	1531,1538

Reference (8 of 20)

Citation Number	3142215
Document Type	Journal
Authors	Banerji; Dhara
CODEN	PYTCAS
Journal Title	Phytochemistry
(Series) Volume	13
Publication Year	1974
Page	2327

Reference (9 of 20)

Citation Number	3142495
Document Type	Journal
Authors	Vashkov et al.
CODEN	RZKHAR
Journal Title	Ref.Zh.Khim.
Journal/Review Without CODEN	Chem.Abstr.
(Series) Volume	17; 81
Number	13234b
Publication Year	1973; 1974
Page	508

Reference (10 of 20)

Citation Number	3214879
Document Type	Journal
Authors	Feugeas
CODEN	BSCFAS
Journal Title	Bull.Soc.Chim.Fr.
Publication Year	1964
Page	1892

Reference (11 of 20)

Citation Number	3220501
Document Type	Journal
Authors	Normant; Feugeas
CODEN	COREAF
Journal Title	C.R.Hebd.Seances Acad.Sci.
(Series) Volume	258
Publication Year	1964
Page	2846

Reference (12 of 20)

Citation Number	3228104
Document Type	Journal
Authors	Graham
CODEN	JPMSAE
Journal Title	J.Pharm.Sci.
(Series) Volume	54
Publication Year	1965
Page	319

Reference (13 of 20)

Citation Number	3239881
Document Type	Journal
Authors	Mishra; Tewari
CODEN	JPMSAE
Journal Title	J.Pharm.Sci.
(Series) Volume	53
Publication Year	1964
Page	1423

Reference (14 of 20)

Citation Number	3281384
Document Type	Journal
Authors	Traxler
CODEN	JAFCAU
Journal Title	J.Agric.Food Chem.
(Series) Volume	19
Publication Year	1971
Page	1135,1137

Reference (15 of 20)

Citation Number	3341233
Document Type	Journal
Authors	Singh et al.
CODEN	JICSAH
Journal Title	J.Indian Chem.Soc.
(Series) Volume	53
Publication Year	1976
Page	1162

Reference (16 of 20)

Citation Number	3633748
Document Type	Journal
Authors	Bohnsack
CODEN	RSARAQ
Journal Title	Riechst.Aromen
(Series) Volume	15
Publication Year	1965
Page	77

Reference (17 of 20)

Citation Number	3678903
Document Type	Journal
Authors	Bordner; Mullins
CODEN	CSCMCS
Journal Title	Cryst.Struct.Commun.
(Series) Volume	3
Publication Year	1974
Page	693

Reference (18 of 20)

Citation Number	4815504
Document Type	Journal
Authors	Kulka
CODEN	JAFCAU
Journal Title	J.Agric.Food Chem.
(Series) Volume	15
Publication Year	1967
Page	48,51

Reference (19 of 20)

Citation Number	5546680
Document Type	Journal
Authors	Mandai, Tadakatsu; Moriyama, Tadashi; Tsujimoto, Koichiro; Kawada, Mikio; Otera, Junzo
CODEN	TELEAY
Journal Title	Tetrahedron Lett.
Language Code	EN
(Series) Volume	27
Number	5
Publication Year	1986
Page	603-606

Reference (20 of 20)

Citation Number	5686470
Document Type	Journal
Authors	Hoelzel, Claus; Spiteller, Gerhard
CODEN	LACHDL
Journal Title	Liebigs Ann.Chem.
Language Code	GE
Number	7
Publication Year	1984
Page	1319-1331

Reaction (1 of 4)

Reaction ID	2627935
Reactant BRN	4613019
Reactant	acetic acid 1-(benzenesulfonyl-benzo[1,3]dioxol-5-yl-methyl)-4-oxo-4-piperidin-1-yl-butyl ester
Product BRN	90739; 90741
Product	1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidine; 1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Reagent	t-BuOK
Solvent	2-methyl-propan-2-ol
Time	12 hour(s)
Other Conditions	Ambient temperature
Comment	Yield given. Yields of byproduct given
Citation Pointer	5546680; Journal; Mandai, Tadakatsu; Moriyama, Tadashi; Tsujimoto, Koichiro; Kawada, Mikio; Otera, Junzo; TELEAY; Tetrahedron Lett.; EN; 27; 5; 1986; 603-606;

Reaction (2 of 4)

Reaction ID	3863768
Reactant BRN	90739
Reactant	1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidine
Product BRN	5564597
Product	5-(3,4-Dihydroxyphenyl)-2,4-pentadiensaeure-piperidid
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	86 percent (BRN=5564597)
Reagent	0.5 M BBr3, 0.5 M sodium acetate buffer (pH=5)
Solvent	CH2Cl2
Time	72 hour(s)
Other Conditions	Ambient temperature
Citation Pointer	5686470; Journal; Hoelzel, Claus; Spiteller, Gerhard; LACHDL; Liebigs Ann.Chem.; GE; 7; 1984; 1319-1331;

Reaction (3 of 4)

Reaction ID	5392514
Reactant BRN	90739
Reactant	1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidine
No. of Reaction Details	2
Reaction Classification	Chemical behaviour (half reaction)
Subject Studied	Kinetics
Citation Pointer	119906; Journal; Stoklosa,K.; BSCFAS; Bull.Soc.Chim.Fr.; FR; 1969; 3802-3806;

Reaction (4 of 4)

Reaction ID	5714783
Product BRN	90739
Product	1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation (half reaction)
Citation Pointer	3220501; Journal; Normant; Feugeas; COREAF; C.R.Hebd.Seances Acad.Sci.; 258; 1964; 2846;3214879; Journal; Feugeas; BSCFAS; Bull.Soc.Chim.Fr.; 1964; 1892;

Isolation from Natural Product (1 of 6)

Isolation from Natural Product	aus Piper nigrum L.
Citation Pointer	3281384; Journal; Traxler; JAFCAU; J.Agric.Food Chem.; 19; 1971; 1135,1137;

Isolation from Natural Product (2 of 6)

Isolation from Natural Product	aus Pfeffer
Citation Pointer	3633748; Journal; Bohnsack; RSARAQ; Riechst.Aromen; 15; 1965; 77;

Isolation from Natural Product (3 of 6)

Isolation from Natural Product	aus Stengel von Piper nigrum Linn.
Citation Pointer	3341233; Journal; Singh et al.; JICSAH; J.Indian Chem.Soc.; 53; 1976; 1162;

Isolation from Natural Product (4 of 6)

Isolation from Natural Product	aus Piper chaba
Citation Pointer	3239881; Journal; Mishra; Tewari; JPMSAE; J.Pharm.Sci.; 53; 1964; 1423;

Isolation from Natural Product (5 of 6)

Isolation from Natural Product	aus Piper longum Linn.
Citation Pointer	3133321; Journal; Dutta et al.; IJSBDB; Indian J.Chem.Sect.B; 15; 1977; 583;

Isolation from Natural Product (6 of 6)

Isolation from Natural Product	aus Piper nepalense
Citation Pointer	2835455; Journal; Gupta et al.; PYTCAS; Phytochemistry; 11; 1972; 2646;

Derivative (1 of 2)

Comment	Hydrobromid: C17H19NO3*HBr: aus Piperin in Bzl., ges. benzol. HBr-Lsg.; F: 170grad
Citation Pointer	3220501; Journal; Normant; Feugeas; COREAF; C.R.Hebd.Seances Acad.Sci.; 258; 1964; 2846;

Derivative (2 of 2)

Comment	Hydrobromid: F: 170grad (aus Bzl.; Kofler-App:)
Citation Pointer	3214879; Journal; Feugeas; BSCFAS; Bull.Soc.Chim.Fr.; 1964; 1892;

Crossfile Reference (1 of 3)

Name	Piperine; for synthesis
Crossfile Source	E.Merck, Darmstadt
External Access ID	821036

Crossfile Reference (2 of 3)

Name	PIPERINE, 97 PERCENT
Crossfile Source	Aldrich
External Access ID	P49007

Crossfile Reference (3 of 3)

Name	piperine
Crossfile Source	EINECS
External Access ID	202-348-0

Melting Point (1 of 9)

Melting Point	129.2 - 130.5
Citation Pointer	3281384; Journal; Traxler; JAFCAU; J.Agric.Food Chem.; 19; 1971; 1135,1137;

Melting Point (2 of 9)

Melting Point	129
Solvent	diethyl ether
Citation Pointer	3220501; Journal; Normant; Feugeas; COREAF; C.R.Hebd.Seances Acad.Sci.; 258; 1964; 2846;3214879; Journal; Feugeas; BSCFAS; Bull.Soc.Chim.Fr.; 1964; 1892;

Melting Point (3 of 9)

Melting Point	128
Citation Pointer	119906; Journal; Stoklosa,K.; BSCFAS; Bull.Soc.Chim.Fr.; FR; 1969; 3802-3806;

Melting Point (4 of 9)

Melting Point	128 - 129.5
Citation Pointer	3142495; Journal; Vashkov et al.; RZKHAR; Ref.Zh.Khim.; 17; 1973; 508; Chem.Abstr.; 81; 13234b; 1974;3633748; Journal; Bohnsack; RSARAQ; Riechst.Aromen; 15; 1965; 77;

Melting Point (5 of 9)

Melting Point	129 - 130
Citation Pointer	2835455; Journal; Gupta et al.; PYTCAS; Phytochemistry; 11; 1972; 2646;

Melting Point (6 of 9)

Melting Point	128 - 129
Citation Pointer	4815504; Journal; Kulka; JAFCAU; J.Agric.Food Chem.; 15; 1967; 48,51;

Melting Point (7 of 9)

Melting Point	127 - 129
Citation Pointer	3142215; Journal; Banerji; Dhara; PYTCAS; Phytochemistry; 13; 1974; 2327;

Melting Point (8 of 9)

Melting Point	128 - 129
Citation Pointer	3133481; Journal; Lurik et al.; JGCHA4; J.Gen.Chem.USSR (Engl.Transl.); 45; 1975; 2246; ZOKHA4; Zh.Obshch.Khim.; 45; 1975; 2287;

Melting Point (9 of 9)

Melting Point	120 - 129
Citation Pointer	3341233; Journal; Singh et al.; JICSAH; J.Indian Chem.Soc.; 53; 1976; 1162;

Crystal Phase (1 of 2)

Description	Crystal habit
Citation Pointer	3678903; Journal; Bordner; Mullins; CSCMCS; Cryst.Struct.Commun.; 3; 1974; 693;

Crystal Phase (2 of 2)

Description	Crystal growth
Citation Pointer	3141536; Journal; Mazeau; Zarzycki; CHDCAQ; C.R.Hebd.Seances Acad.Sci.Ser.C; 281; 1975; 583,584;

Nuclear Magnetic Resonance (1 of 1)

Description	NMR
Citation Pointer	3133481; Journal; Lurik et al.; JGCHA4; J.Gen.Chem.USSR (Engl.Transl.); 45; 1975; 2246; ZOKHA4; Zh.Obshch.Khim.; 45; 1975; 2287;

Infrared Spectra (1 of 1)

Description	IR
Citation Pointer	3133481; Journal; Lurik et al.; JGCHA4; J.Gen.Chem.USSR (Engl.Transl.); 45; 1975; 2246; ZOKHA4; Zh.Obshch.Khim.; 45; 1975; 2287;3142215; Journal; Banerji; Dhara; PYTCAS; Phytochemistry; 13; 1974; 2327;3220501; Journal; Normant; Feugeas; COREAF; C.R.Hebd.Seances Acad.Sci.; 258; 1964; 2846;

Ultraviolet Spectra (1 of 2)

Description	Absorption maxima
Citation Pointer	3220501; Journal; Normant; Feugeas; COREAF; C.R.Hebd.Seances Acad.Sci.; 258; 1964; 2846;

Ultraviolet Spectra (2 of 2)

Description	UV/VIS
Citation Pointer	3133481; Journal; Lurik et al.; JGCHA4; J.Gen.Chem.USSR (Engl.Transl.); 45; 1975; 2246; ZOKHA4; Zh.Obshch.Khim.; 45; 1975; 2287;3281384; Journal; Traxler; JAFCAU; J.Agric.Food Chem.; 19; 1971; 1135,1137;

Mass Spectrum (1 of 1)

Citation Pointer

3142215; Journal; Banerji; Dhara; PYTCAS; Phytochemistry; 13; 1974; 2327;

Electrochemical Characteristics (1 of 1)

Description	polarographic half-wave potential
Citation Pointer	3133481; Journal; Lurik et al.; JGCHA4; J.Gen.Chem.USSR (Engl.Transl.); 45; 1975; 2246; ZOKHA4; Zh.Obshch.Khim.; 45; 1975; 2287;

Further Information (1 of 2)

Citation Pointer

3141959; Journal; Loder et al.; AJCHAS; Aust.J.Chem.; 22; 1969; 1531,1538;3228104; Journal; Graham; JPMSAE; J.Pharm.Sci.; 54; 1965; 319;

Further Information (2 of 2)

Citation Pointer

2605306; Journal; Lloyd et al.; JACSAT; J.Amer.Chem.Soc.; 82; 1960; 3791;

Hit 2

FA	IDE(1); FLST(23); XREF(4); RSTR(1); INP(30); CDER(1); CPD(2); MP(19); CRYPH(8); SP(1); DEN(4); DV(1); RI(1); NMR(15); IR(12); UV(10); MS(5); ELE(1); DE(3); POT(1); SLB(8); BSPM(1); PHARM(60); RX(31); CNR(126)

Substance (1 of 1)

Beilstein Registry Number	90741
Beilstein Preferred RN	94-62-2
CAS Registry Number	94-62-2; 495-91-0; 7780-20-3; 30511-76-3; 30511-77-4
Chemical Name	1-trans,trans-piperinoyl-piperidine; piperine; (E,E)-1-[5-(1,3-benzodioxol-5-yl)-1-oxo-2,4-pentadienyl]-piperidine
Autoname	5-benzo[1,3]dioxol-5-yl-1-piperidin-1-yl-penta-2,4-dien-1-one
Molecular Formula	C17H19NO3
Molecular Weight	285.34
Lawson Number	24081; 22876
Structure Keyword	Stereo compound
Compound Type	heterocyclic
Constitution ID	38159
Tautomer ID	18563
Beilstein Reference	0-20-00-00079; 1-20-00-00023; 2-20-00-00053; 4-20-00-01341; 5-20-03-00469; 6-20
Entry Date	1988/06/27
Update Date	2002/04/29

Reference (1 of 126)

Citation Number	156361
Document Type	Journal
Authors	Okogun,J.I.; Ekong,D.E.U.
CODEN	JCPRB4
Journal Title	J.Chem.Soc.Perkin Trans.1
Language Code	EN
Publication Year	1974
Page	2195-2198

Reference (2 of 126)

Citation Number	502948
Document Type	Journal
Authors	Peinemann
CODEN	ARPMAS
Journal Title	Arch.Pharm.(Weinheim Ger.)
(Series) Volume	234
Publication Year	1896
Page	258

Reference (3 of 126)

Citation Number	503101
Document Type	Journal
Authors	Fittig; Mielck
CODEN	JLACBF; JLACBF
Journal Title	Justus Liebigs Ann. Chem.; Justus Liebigs Ann. Chem.
(Series) Volume	152; 172
Publication Year	1869; 1874
Page	52, 54; 140, 152

Reference (4 of 126)

Citation Number	505033
Document Type	Journal
Authors	Borsche
CODEN	CHBEAM
Journal Title	Chem.Ber.
(Series) Volume	44
Publication Year	1911
Page	2945

Reference (5 of 126)

Citation Number	505376
Document Type	Journal
Authors	Dehn
CODEN	JACSAT
Journal Title	J.Amer.Chem.Soc.
(Series) Volume	39
Publication Year	1917
Page	1400

Reference (6 of 126)

Citation Number	505581
Document Type	Journal
Authors	Dobbie; Fox
CODEN	JCSOA9
Journal Title	J.Chem.Soc.
(Series) Volume	103
Publication Year	1913
Page	1194

Reference (7 of 126)

Citation Number	507531
Document Type	Journal
Authors	Lohaus
CODEN	JPCEAO
Journal Title	J.Prakt.Chem.
(Series) Volume	<2> 119
Publication Year	1928
Page	258

Reference (8 of 126)

Citation Number	511899
Document Type	Journal
Authors	Briggs et al.
CODEN	ANCHAM
Journal Title	Anal.Chem.
(Series) Volume	29
Publication Year	1957
Page	904, 905

Reference (9 of 126)

Citation Number	520054
Document Type	Journal
Authors	Lohaus; Gall
CODEN	JLACBF
Journal Title	Justus Liebigs Ann. Chem.
(Series) Volume	517
Publication Year	1935
Page	278, 284

Reference (10 of 126)

Citation Number	529237
Document Type	Journal
Authors	Spring; Stark
CODEN	JCSOA9
Journal Title	J.Chem.Soc.
Publication Year	1950
Page	1177, 1178

Reference (11 of 126)

Citation Number	536898
Document Type	Journal
Authors	Kopzik et al.
CODEN	VMUNAE
Journal Title	Vestn.Mosk.Univ.
Journal/Review Without CODEN	Chem.Abstr.
(Series) Volume	13
Number	6
Publication Year	1958; 1959
Page	91, 94; 15673

Reference (12 of 126)

Citation Number	559145
Document Type	Journal
Authors	Wester
CODEN	CHZEA6
Journal Title	Chem.Zentralbl.
Language Code	GE
(Series) Volume	86
Number	I
Publication Year	1915
Page	248

Reference (13 of 126)

Citation Number	562634
Document Type	Journal
Authors	Pucher; Dehn
CODEN	JACSAT
Journal Title	J.Amer.Chem.Soc.
(Series) Volume	43
Publication Year	1921
Page	1755

Reference (14 of 126)

Citation Number	621663
Document Type	Journal
Authors	Skita; Franck
CODEN	CHBEAM
Journal Title	Chem.Ber.
(Series) Volume	44
Publication Year	1911
Page	2866

Reference (15 of 126)

Citation Number	625129
Document Type	Journal
Authors	Arnall
CODEN	JCSOA9
Journal Title	J.Chem.Soc.
(Series) Volume	117
Publication Year	1920
Page	837

Reference (16 of 126)

Citation Number	625734
Document Type	Journal
Authors	v. Weisse; Meyer-Levy
CODEN	JCPBAN; CHZEA6
Journal Title	J.Chim.Phys.Phys.Chim.Biol.; Chem.Zentralbl.
Language Code	GE
(Series) Volume	14; 87
Number	II
Publication Year	1916; 1916
Page	276; 1030

Reference (17 of 126)

Citation Number	625737
Document Type	Journal
Authors	Zeehuisen
CODEN	AEPPAE; CHZEA6
Journal Title	Naunyn-Schmiedeberg's Arch.Exp.Pathol.Pharmakol.; Chem.Zentralbl.
Language Code	GE
(Series) Volume	86; 91
Number	III
Publication Year	1920; 1920
Page	366; 668

Reference (18 of 126)

Citation Number	636409
Document Type	Journal
Authors	Janot; Chaigneau
CODEN	COREAF
Journal Title	C.R.Hebd.Seances Acad.Sci.
(Series) Volume	225
Publication Year	1947
Page	1371

Reference (19 of 126)

Citation Number	642911
Document Type	Journal
Authors	Pleat et al.
CODEN	JPHAA3
Journal Title	J.Am.Pharm.Assoc.
(Series) Volume	40
Publication Year	1951
Page	107, 108

Reference (20 of 126)

Citation Number	740972
Document Type	Journal
Authors	Kolthoff
CODEN	BIZEA2; PHJOAV; CHZEA6
Journal Title	Biochem.Z.; Pharm.J.; Chem.Zentralbl.
Language Code	GE
(Series) Volume	162; 118; 98
Number	I
Publication Year	1925; 1927
Page	340; 126; 2116

Reference (21 of 126)

Citation Number	745868
Document Type	Journal
Authors	Paterno
CODEN	GCITA9
Journal Title	Gazz.Chim.Ital.
(Series) Volume	44 II
Publication Year	1914
Page	104, 106

Reference (22 of 126)

Citation Number	784769
Document Type	Patent
Patent Author	Lever Brothers Co.
Patent Number	US 2085064
Patent Year	1935

Reference (23 of 126)

Citation Number	960841
Document Type	Journal
Authors	v. Babo; Keller
CODEN	JPCEAO; JCVWAE
Journal Title	J.Prakt.Chem.; Jahresber.Fortschr.Chem.Verw.Theile Anderer Wiss.
(Series) Volume	<1> 72
Publication Year	1857; 1857
Page	55; 413

Reference (24 of 126)

Citation Number	960844
Document Type	Journal
Authors	Ruegheimer
CODEN	CHBEAM
Journal Title	Chem.Ber.
(Series) Volume	15
Publication Year	1882
Page	1391

Reference (25 of 126)

Citation Number	960845
Document Type	Journal
Authors	Peckolt
Journal/Review Without CODEN	Apoth. Ztg.
(Series) Volume	10
Page	471

Reference (26 of 126)

Citation Number	960846
Document Type	Journal
Authors	Herlant
CODEN	PHJOAV
Journal Title	Pharm.J.
(Series) Volume	<3> 25
Page	643

Reference (27 of 126)

Citation Number	960847
Document Type	Journal
Authors	Stenhouse
CODEN	PHJOAV; JLACBF
Journal Title	Pharm.J.; Justus Liebigs Ann. Chem.
(Series) Volume	<1> 14; 95
Publication Year	1855
Page	363; 106

Reference (28 of 126)

Citation Number	960848
Document Type	Journal
Authors	Wangerin
Journal/Review Without CODEN	Pharm. Ztg.
(Series) Volume	48
Page	454

Reference (29 of 126)

Citation Number	960849
Document Type	Journal
Authors	Bauer; Hilger
CODEN	CHZEA6
Journal Title	Chem.Zentralbl.
Language Code	GE
(Series) Volume	67
Number	I
Publication Year	1896
Page	1214

Reference (30 of 126)

Citation Number	960850
Document Type	Journal
Authors	Varrentrapp; Will
CODEN	JLACBF
Journal Title	Justus Liebigs Ann. Chem.
(Series) Volume	39
Publication Year	1841
Page	283

Reference (31 of 126)

Citation Number	960851
Document Type	Journal
Authors	Regnault
CODEN	ANCPAC
Journal Title	Ann.Chim.(Paris)
(Series) Volume	<2> 68
Publication Year	1838
Page	158

Reference (32 of 126)

Citation Number	960852
Document Type	Journal
Authors	Liebig
CODEN	JLACBF
Journal Title	Justus Liebigs Ann. Chem.
(Series) Volume	6
Publication Year	1833
Page	36

Reference (33 of 126)

Citation Number	960853
Document Type	Journal
Authors	Pelletier
CODEN	ANCPAC; JLACBF
Journal Title	Ann.Chim.(Paris); Justus Liebigs Ann. Chem.
(Series) Volume	<2> 51; 6
Publication Year	1832; 1833
Page	199; 33

Reference (34 of 126)

Citation Number	960854
Document Type	Journal
Authors	Pelletier
CODEN	ANCPAC
Journal Title	Ann.Chim.(Paris)
Journal/Review Without CODEN	Schw.
(Series) Volume	<2> 16; 32
Publication Year	1821
Page	344; 436

Reference (35 of 126)

Citation Number	960855
Document Type	Journal
Authors	Oerstedt
Journal/Review Without CODEN	Schweiggers Journ. f. Chemie u. Physik
(Series) Volume	29
Page	80

Reference (36 of 126)

Citation Number	967599
Document Type	Journal
Authors	Skita; Meyer
CODEN	CHBEAM
Journal Title	Chem.Ber.
(Series) Volume	45
Publication Year	1912
Page	3586

Reference (37 of 126)

Citation Number	967610
Document Type	Journal
Authors	Tunmann
CODEN	CHZEA6
Journal Title	Chem.Zentralbl.
Language Code	GE
(Series) Volume	89
Number	II
Publication Year	1918
Page	675

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Citation Number	6303567
Document Type	Journal
Authors	Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.
CODEN	PLMEAA
Journal Title	Planta Med.
Language Code	EN
(Series) Volume	67
Number	2
Publication Year	2001
Page	176 - 179

Reference (123 of 126)

Citation Number	6303601
Document Type	Journal
Authors	Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.
CODEN	PLMEAA
Journal Title	Planta Med.
Language Code	EN
(Series) Volume	67
Number	3
Publication Year	2001
Page	284 - 287

Reference (124 of 126)

Citation Number	6311443
Document Type	Journal
Authors	Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.
CODEN	JCSPCE
Journal Title	J.Chem.Soc.Perkin Trans.1
Language Code	EN
Number	19
Publication Year	2001
Page	2393 - 2397

Reference (125 of 126)

Citation Number	6318024
Document Type	Journal
Authors	Sunkara, G.; Mada, S. R.; Vobalaboina, V.
CODEN	PHARAT
Journal Title	Pharmazie
Language Code	EN
(Series) Volume	56
Number	8
Publication Year	2001
Page	640 - 642

Reference (126 of 126)

Citation Number	6320341
Document Type	Journal
Authors	Grainger, Richard S.; Procopio, Alberto; Steed, Jonathan W.
CODEN	ORLEF7
Journal Title	Org.Lett.
Language Code	EN
(Series) Volume	3
Number	22
Publication Year	2001
Page	3565 - 3568

Reaction (1 of 31)

Reaction ID	1746488
Reactant BRN	4327482; 1310620
Reactant	2-(3,6-diisopropyl-pyrazine-2-sulfinyl)-1-piperidin-1-yl-ethanone; 5-(3-bromo-1-propenyl)-1,3-dioxaindan
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Reagent	1.) potassium diisopropylamide (KDA)
Other Conditions	1.) THF, hexane, RT, 1 h, 2.) THF, hexane, reflux
Comment	Yield given. Multistep reaction
Citation Pointer	5535863; Journal; Ohta, Akihiro; Tonomura, Yoshiko; Sawaki, Junko; Naohito, Sato; Akiike, Hitomi; et al.; HTCYAM; Heterocycles; EN; 32; 5; 1991; 965-973;

Reaction (2 of 31)

Reaction ID	1748676
Reactant BRN	1365055; 131691
Reactant	N-2-butenoylpiperidine; benzo[1,3]dioxole-5-carbaldehyde
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	3
Reaction Classification	Chemical behaviour
Reagent	triethylbenzylammoniumchloride, 50percent KOH
Solvent	dimethylsulfoxide
Time	2 hour(s)
Temperature	60 - 65
Other Conditions	various solvents
Subject Studied	Product distribution
Citation Pointer	5623047; Journal; Schulze, Andreas; Oediger, Hermann; LACHDL; Liebigs Ann.Chem.; GE; 9; 1981; 1725-1727;

Reaction (3 of 31)

Reaction ID	1839034
Reactant BRN	167676; 4416084
Reactant	1-benzo[1,3]dioxol-5-yl-allyl alcohol; 1-p-tolylsulfanylethynyl-piperidine
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Other Conditions	1.) BF3OEt2 in refluxing toluene; 2.) oxidation (m-chloroperbenzoic acid, CH2Cl2,-78 grad C); 3.) reflux in toluene
Comment	Yield given. Multistep reaction
Citation Pointer	5542826; Journal; Nakai, Takeshi; Setoi, Hiroyuki; Kageyama, Yasuhide; TELEAY; Tetrahedron Lett.; EN; 22; 41; 1981; 4097-4100;

Reaction (4 of 31)

Reaction ID	2627935
Reactant BRN	4613019
Reactant	acetic acid 1-(benzenesulfonyl-benzo[1,3]dioxol-5-yl-methyl)-4-oxo-4-piperidin-1-yl-butyl ester
Product BRN	90739; 90741
Product	1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidine; 1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Reagent	t-BuOK
Solvent	2-methyl-propan-2-ol
Time	12 hour(s)
Other Conditions	Ambient temperature
Comment	Yield given. Yields of byproduct given
Citation Pointer	5546680; Journal; Mandai, Tadakatsu; Moriyama, Tadashi; Tsujimoto, Koichiro; Kawada, Mikio; Otera, Junzo; TELEAY; Tetrahedron Lett.; EN; 27; 5; 1986; 603-606;

Reaction (5 of 31)

Reaction ID	3829573
Reactant BRN	85624; 102438
Reactant	trans,trans-piperinic acid; piperidine
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	2
Reaction Classification	Preparation
Yield	90 percent (BRN=90741)
Reagent	N,N-bis(2-oxo-3-oxazolidinyl)phosphorodiamidic chloride, triethylamine
Solvent	CH2Cl2
Time	60 min
Temperature	20 - 25
Citation Pointer	5571390; Journal; Cabre, Juan; Palomo, Antonio Luis; SYNTBF; Synthesis; EN; 5; 1984; 413-417;

Reaction (6 of 31)

Reaction ID	3829578
Reactant BRN	85625; 102438
Reactant	5t-benzo[1,3]dioxol-5-yl-penta-2t,4-dienoyl chloride; piperidine
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	2
Reaction Classification	Preparation
Solvent	diethyl ether
Citation Pointer	5576619; Journal; Banerji, Avijit; Ghosal, Tapasree; Acharyya, Aditi K.; IJSBDB; Indian J.Chem.Sect.B; EN; 23; 6; 1984; 546-549;

Reaction (7 of 31)

Reaction ID	3863772
Reactant BRN	1101343; 90741
Reactant	chloromalonic acid diethyl ester; 1-trans,trans-piperinoyl-piperidine
Product BRN	1805352; 4894122
Product	ethenetetracarboxylic acid tetraethyl ester; 3-benzo[1,3]dioxol-5-yl-6-(piperidine-1-carbonyl)-3,6-dihydro-selenopyran-2,2-dicarboxylic acid diethyl ester
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	24 percent (BRN=4894122); 70 percent (BRN=1805352)
Reagent	selenium, Cs2CO3
Solvent	acetonitrile
Other Conditions	Heating
Citation Pointer	5597332; Journal; Abelman, Matthew M.; TELEAY; Tetrahedron Lett.; EN; 32; 50; 1991; 7389-7392;

Reaction (8 of 31)

Reaction ID	3863773
Reactant BRN	1101343; 90741
Reactant	chloromalonic acid diethyl ester; 1-trans,trans-piperinoyl-piperidine
Product BRN	4894108
Product	3-benzo[1,3]dioxol-5-yl-6-(piperidine-1-carbonyl)-3,6-dihydro-thiopyran-2,2-dicarboxylic acid diethyl ester
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	80 percent (BRN=4894108)
Reagent	sulfur, Cs2CO3
Solvent	acetonitrile
Other Conditions	Heating
Citation Pointer	5597332; Journal; Abelman, Matthew M.; TELEAY; Tetrahedron Lett.; EN; 32; 50; 1991; 7389-7392;

Reaction (9 of 31)

Reaction ID	3863774
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	110253
Product	1-nitroso-piperidine
No. of Reaction Details	2
Reaction Classification	Preparation
Yield	2.36 percent (BRN=110253)
Reagent	HClO4 (pH 3.0), NaNO2
Solvent	H2O
Time	2 hour(s)
Temperature	100
Citation Pointer	5874363; Journal; Nakamura, Masamichi; Katoh, Kuni; Kawabata, Toshiharu; ABCHA6; Agric.Biol.Chem.; EN; 45; 5; 1981; 1257-1260;

Reaction (10 of 31)

Reaction ID	3863775
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	288703
Product	1-(5-benzo[1,3]dioxol-5-yl-pentanoyl)-piperidine
No. of Reaction Details	4
Reaction Classification	Preparation
Reagent	H2
Catalyst	10 percent Pd/C
Solvent	methanol
Time	2 hour(s)
Pressure	2585.74
Reaction Type	Catalytic hydrogenation
Citation Pointer	6262921; Journal; Ablordeppey, Seth Y.; Fischer, James B.; Glennon, Richard A.; BMECEP; Bioorg.Med.Chem.; EN; 8; 8; 2000; 2105 - 2112;

Reaction (11 of 31)

Reaction ID	3863776
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	6144494; 6168367
Product	Z-5-benzylidene-(3,4-methylenedioxy)-2(5H)-furanone; E,E-piperylpiperidine dimer
No. of Reaction Details	3
Reaction Classification	Chemical behaviour
Yield	26 percent (BRN=6144494); 30 percent (BRN=6168367)
Reagent	rose bengal
Solvent	methanol
Time	18 hour(s)
Other Conditions	Irradiation
Subject Studied	Mechanism
Citation Pointer	5753488; Journal; Kumar, Anil; Krupadanam, G L David; Srimannarayana, G; IJSBDB; Indian J.Chem.Sect.B; EN; 31; 11; 1992; 784-785;

Reaction (12 of 31)

Reaction ID	3863777
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	6662570
Product	4,5-(trans)-2,3-epoxy piperylpiperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	75 percent (BRN=6662570)
Reagent	1percent H2O2
Time	18 hour(s)
Temperature	37
Other Conditions	Horseradish peroxidase, 0,1M sodium phosphate buffer, pH 6,5
Citation Pointer	5851492; Journal; Rao, A. Bhaskar; Rao, M. Venkateswara; Kumar, Anil; Krupadanam, G. L. David; Srimannarayana, G.; TELEAY; Tetrahedron Lett.; EN; 35; 2; 1994; 279-280;

Reaction (13 of 31)

Reaction ID	3863778
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	85624
Product	trans,trans-piperinic acid
No. of Reaction Details	3
Reaction Classification	Preparation
Reagent	10percent ethanolic NaOH
Solvent	ethanol
Citation Pointer	5725528; Journal; Nakamura, Norio; Kiuchi, Fumiyuki; Tsuda, Yoshisuke; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2647-2651;

Reaction (14 of 31)

Reaction ID	4925582
Reactant BRN	7989620; 114442
Reactant	5-(2-iodo-vinyl)-benzo[1,3]dioxole; 1-acryloyl-piperidine
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	38 percent (BRN=90741)
Reagent	palladium acetate, triphenylphosphine, lithium chloride, triethylamine
Solvent	acetonitrile
Time	18 hour(s)
Temperature	70 - 80
Citation Pointer	6096589; Journal; Naskar, Dinabandhu; Chowdhury, Shantanu; Roy, Sujit; TELEAY; Tetrahedron Lett.; EN; 39; 7; 1998; 699-702;

Reaction (15 of 31)

Reaction ID	4975527
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	8003486; 288703
Product	5-benzo[1,3]dioxol-5-yl-1-piperidin-1-yl-pent-4-en-1-one; 1-(5-benzo[1,3]dioxol-5-yl-pentanoyl)-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	58 percent (BRN=288703); 14 percent (BRN=8003486)
Reagent	NaBH4 (0.008 mole), I2 (0.003 mole)
Solvent	tetrahydrofuran
Time	20 min
Temperature	0
Citation Pointer	6096582; Journal; Das, Biswanath; Kashinatham, A.; Madhusudhan, P.; TELEAY; Tetrahedron Lett.; EN; 39; 7; 1998; 677-678;

Reaction (16 of 31)

Reaction ID	4975528
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	8003486
Product	5-benzo[1,3]dioxol-5-yl-1-piperidin-1-yl-pent-4-en-1-one
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	74 percent (BRN=8003486)
Reagent	NaBH4 (0.0025 mole), I2 (0.001 mole)
Solvent	tetrahydrofuran
Time	20 min
Temperature	0
Citation Pointer	6096582; Journal; Das, Biswanath; Kashinatham, A.; Madhusudhan, P.; TELEAY; Tetrahedron Lett.; EN; 39; 7; 1998; 677-678;

Reaction (17 of 31)

Reaction ID	5043968
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	8117956; 1261487
Product	5-benzo[1,3]dioxol-5-yl-1-piperidin-1-yl-pent-3-en-1-one; trans-Db,g-Dihydro-piperidin
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	95 percent (BRN=1261487)
Reagent	Zn, HOAc
Time	2 hour(s)
Other Conditions	Ambient temperature
Citation Pointer	6117787; Journal; Das, Biswanath; Madhusudhan, P.; TELEAY; Tetrahedron Lett.; EN; 39; 49; 1998; 9099-9100;

Reaction (18 of 31)

Reaction ID	5311563
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	1261487
Product	trans-Db,g-Dihydro-piperidin
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	96 percent (BRN=1261487)
Reagent	Mg; MeOH
Time	2 hour(s)
Temperature	20
Reaction Type	Reduction
Citation Pointer	6209404; Journal; Das, Biswanth; Kashinatham, A.; Venkataiah, B.; SYNCAV; Synth.Commun.; EN; 29; 21; 1999; 3799 - 3804;

Reaction (19 of 31)

Reaction ID	5392515
Reactant BRN	1238185; 90741
Reactant	benzophenone; 1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Chemical behaviour (half reaction)
Other Conditions	im Licht
Comment	Handbook
Citation Pointer	745868; Journal; Paterno; GCITA9; Gazz.Chim.Ital.; 44 II; 1914; 104, 106;

Reaction (20 of 31)

Reaction ID	5680972
Reactant BRN	90741; 1718733
Reactant	1-trans,trans-piperinoyl-piperidine; ethanol; phenylmercury-acetate
Product BRN	53813
Product	1-[5t-(6-phenylmercurio-benzo[1,3]dioxol-5-yl)-penta-2t,4-dienoyl]-piperidine
No. of Reaction Details	2
Reaction Classification	Preparation
Comment	Handbook
Citation Pointer	784769; Patent; Lever Brothers Co.; US 2085064; 1935;

Reaction (21 of 31)

Reaction ID	5709607
Reactant BRN	90741
Reactant	alcoholic KOH-solution; 1-trans,trans-piperinoyl-piperidine
Product BRN	102438; 85624
Product	piperidine; trans,trans-piperinic acid
No. of Reaction Details	1
Reaction Classification	Chemical behaviour
Comment	Handbook
Citation Pointer	960841; Journal; v. Babo; Keller; JPCEAO; J.Prakt.Chem.; <1> 72; 1857; 55; JCVWAE; Jahresber.Fortschr.Chem.Verw.Theile Anderer Wiss.; 1857; 413;503101; Journal; Fittig; Mielck; JLACBF; Justus Liebigs Ann. Chem.; 152; 1869; 52, 54; JLACBF; Justus Liebigs Ann. Chem.; 172; 1874; 140, 152;

Reaction (22 of 31)

Reaction ID	5714786
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation (half reaction)
Citation Pointer	3132215; Journal; Tsuboi; Takeda; TELEAY; Tetrahedron Lett.; 1979; 1043;3140982; Journal; Grewe et al.; CHBEAM; Chem.Ber.; 103; 1970; 3752,3766;3141492; Journal; Lurik et al.; PCJOAU; Pharm.Chem.J.(Engl.Transl.); 5; 8; 1971; 462; KHFZAN; Khim.Farm.Zh.; 5; 8; 1971; 15;2995721; Patent; Haarmann and Reimer; DE 2757506; 1977;

Reaction (23 of 31)

Reaction ID	5714787
Reactant BRN	102438
Reactant	chavicinoyl chloride; piperidine
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Comment	Handbook
Citation Pointer	520054; Journal; Lohaus; Gall; JLACBF; Justus Liebigs Ann. Chem.; 517; 1935; 278, 284;507531; Journal; Lohaus; JPCEAO; J.Prakt.Chem.; <2> 119; 1928; 258;

Reaction (24 of 31)

Reaction ID	5714788
Reactant BRN	102438
Reactant	piperidine; piperinic acid chloride
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Reagent	benzene
Comment	Handbook
Citation Pointer	960844; Journal; Ruegheimer; CHBEAM; Chem.Ber.; 15; 1882; 1391;

Reaction (25 of 31)

Reaction ID	5746581
Reactant BRN	1718733; 90741
Reactant	ethanol; hydrogen; colloidal palladium; 1-trans,trans-piperinoyl-piperidine
Product	tetrahydropiperine
No. of Reaction Details	1
Reaction Classification	Chemical behaviour (half reaction)
Comment	Handbook
Citation Pointer	505033; Journal; Borsche; CHBEAM; Chem.Ber.; 44; 1911; 2945;967599; Journal; Skita; Meyer; CHBEAM; Chem.Ber.; 45; 1912; 3586;1310037; Journal; Paal; CHBEAM; Chem.Ber.; 45; 1912; 2226;

Reaction (26 of 31)

Reaction ID	5746582
Reactant BRN	1098214; 90741
Reactant	hydrogen; hydrochloric acid; palladium chloride; 1-trans,trans-piperinoyl-piperidine
Product	tetrahydropiperine
No. of Reaction Details	1
Reaction Classification	Chemical behaviour (half reaction)
Comment	Handbook
Citation Pointer	621663; Journal; Skita; Franck; CHBEAM; Chem.Ber.; 44; 1911; 2866;

Reaction (27 of 31)

Reaction ID	5746583
Reactant BRN	1098214; 90741
Reactant	hydrogen; hydrochloric acid; platinum chlorides; 1-trans,trans-piperinoyl-piperidine
Product	tetrahydropiperine
No. of Reaction Details	1
Reaction Classification	Chemical behaviour (half reaction)
Comment	Handbook
Citation Pointer	621663; Journal; Skita; Franck; CHBEAM; Chem.Ber.; 44; 1911; 2866;

Reaction (28 of 31)

Reaction ID	8539764
Reactant BRN	84600; 114442
Reactant	3-benzo[1,3]dioxol-5-yl-acrylic acid; 1-acryloyl-piperidine
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Multistage
Yield	51 percent (BRN=90741)
No. of Stages	2
Stage 1
Stage 2
Stage Reactant BRN	114442
Stage Reactant	1-acryloyl-piperidine
Reagent	N-bromosuccinimide; tetrabutylammonium trifluoroacetate; Pd(OAc)2; Ph3Sb; Et3N
Solvent	1,2-dichloro-ethane; 1,2-dichloro-ethane
Time	4 hour(s); 20 hour(s)
Temperature	20
Reaction Type	Decarboxylation; bromination; Hunsdiecker reaction; Heck reaction
Citation Pointer	6225104; Journal; Naskar, Dinabandhu; Roy, Sujit; TETRAB; Tetrahedron; EN; 56; 10; 2000; 1369 - 1378;

Reaction (29 of 31)

Reaction ID	8735157
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	8705257
Product	1-[1-(3,4-methylenedioxyphenyl)-2,4-pentadienyl]piperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Reagent	LiAlH4
Solvent	diethyl ether
Time	24 hour(s)
Other Conditions	Heating
Reaction Type	Reduction
Citation Pointer	6262921; Journal; Ablordeppey, Seth Y.; Fischer, James B.; Glennon, Richard A.; BMECEP; Bioorg.Med.Chem.; EN; 8; 8; 2000; 2105 - 2112;

Reaction (30 of 31)

Reaction ID	8900343
Reactant BRN	7622; 2811397; 102438
Reactant	3,4-methylenedioxy-trans-cinnamaldehyde; (triphenylphosphoranylidene)ethenone; piperidine
Product BRN	90741
Product	1-trans,trans-piperinoyl-piperidine
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	90 percent (BRN=90741)
Solvent	tetrahydrofuran
Time	24 hour(s)
Other Conditions	Heating
Citation Pointer	6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 - 2397;

Reaction (31 of 31)

Reaction ID	8986873
Reactant BRN	90741
Reactant	1-trans,trans-piperinoyl-piperidine
Product BRN	8998762
Product	(5-benzo[1,3]dioxol-5-yl-thiophen-2-yl)-piperidin-1-yl-methanone
No. of Reaction Details	1
Reaction Classification	Preparation
Yield	23 percent (BRN=8998762)
Reagent	naphthalene-1,8-trisulfide-2-oxide
Solvent	chlorobenzene
Time	16 hour(s)
Other Conditions	Heating
Citation Pointer	6320341; Journal; Grainger, Richard S.; Procopio, Alberto; Steed, Jonathan W.; ORLEF7; Org.Lett.; EN; 3; 22; 2001; 3565 - 3568;

Isolation from Natural Product (1 of 30)

Isolation from Natural Product	oleoresin, extract from fruits of Piper nigrum L. (Piperaceae)
Citation Pointer	6303567; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 2; 2001; 176 - 179;

Isolation from Natural Product (2 of 30)

Isolation from Natural Product	stems of Piper tuberculatum
Citation Pointer	6264052; Journal; Navickiene, Hosana Maria D.; Alecio, Alberto Camilo; Kato, Massuo Jorge; Bolzani, Vanderlan da S.; Young, Maria Claudia M.; Cavalheiro, Alberto Jose; Furlan, Maysa; PYTCAS; Phytochemistry; EN; 55; 2410; 2000; 621 - 626;

Isolation from Natural Product (3 of 30)

Isolation from Natural Product	dry fruits of black pepper
Citation Pointer	6225880; Journal; Paula, Vanderlucia F. de; A Barbosa, Luiz C. de; Demuner, Antonio J.; Pilo-Veloso, Dorila; Picanco, Marcelo C.; PMSCFC; Post Manage.Sci.; EN; 56; 2; 2000; 168 - 174;

Isolation from Natural Product (4 of 30)

Isolation from Natural Product	fruits of Piper retrofractum Vahl.
Citation Pointer	6205590; Journal; Pande, Archana; Shukla, Y. N.; Srivastava, Ritu; Verma, Monika; IJSBDB; Indian J.Chem.Sect.B; EN; 36; 4; 1997; 377 - 379;

Isolation from Natural Product (5 of 30)

Isolation from Natural Product	the fruits of Piper Longum Linn (Piperaceae)
Citation Pointer	6161595; Journal; Das, B.; Kashinatham, A.; Madhusudhan, P.; BCFAAI; Boll.Chim.Farm.; EN; 137; 8; 1998; 319 - 320;

Isolation from Natural Product (6 of 30)

Isolation from Natural Product	leaves of Piper betle
Citation Pointer	6124808; Journal; Parmar, Virinder S.; Jain, Subhash C.; Gupta, Sangita; Talwar, Sangeeta; Rajwanshi, Vivek K.; et al.; PYTCAS; Phytochemistry; EN; 49; 4; 1998; 1069-1078;

Isolation from Natural Product (7 of 30)

Isolation from Natural Product	stems and leaves of Piper khasiana, Piper thomsoni, Piper acutislegnum
Citation Pointer	6124808; Journal; Parmar, Virinder S.; Jain, Subhash C.; Gupta, Sangita; Talwar, Sangeeta; Rajwanshi, Vivek K.; et al.; PYTCAS; Phytochemistry; EN; 49; 4; 1998; 1069-1078;

Isolation from Natural Product (8 of 30)

Isolation from Natural Product	Piper acutisleginum, Piperle, Piper khasiana
Citation Pointer	6080863; Journal; Parmar, Virinder S.; Jain, Subhash C.; Bisht, Kirpal S.; Jain, Pajni; Taneja, Poonam; et al.; PYTCAS; Phytochemistry; EN; 46; 4; 1997; 597-674;

Isolation from Natural Product (9 of 30)

Isolation from Natural Product	fruits of Piper nigrum
Citation Pointer	6070238; Journal; Siddiqui, Bina S.; Begum, Sabira; Gulzar, Tahsin; Noor, Farhat and Fatima; PYTCAS; Phytochemistry; EN; 45; 8; 1997; 1617-1620;

Isolation from Natural Product (10 of 30)

Isolation from Natural Product	fruits of Piper longum L. (Piperaceae), climber from India
Citation Pointer	6049858; Journal; Das, Biswanath; Kashinatham, A.; Srinivas, K. V. N. S.; PLMEAA; Planta Med.; EN; 62; 6; 1996; 582;

Isolation from Natural Product (11 of 30)

Isolation from Natural Product	black pepper at 294 bar and 42 deg C, extracted with CO2
Citation Pointer	5945187; Journal; Braumann, Urich; Haendel, heidrun; Albert, Klaus; Ecker, Rainer; Spraul, Manfred; ANCHAM; Anal.Chem.; EN; 67; 5; 1995; 930-935;

Isolation from Natural Product (12 of 30)

Isolation from Natural Product	fruits of white pepper (Piper nigrum L.)
Citation Pointer	5874394; Journal; Nakatani, Nobuji; Inatani, Reiko; ABCHA6; Agric.Biol.Chem.; EN; 45; 6; 1981; 1473-1476;

Isolation from Natural Product (13 of 30)

Isolation from Natural Product	Piper nigrum L.
Citation Pointer	5874363; Journal; Nakamura, Masamichi; Katoh, Kuni; Kawabata, Toshiharu; ABCHA6; Agric.Biol.Chem.; EN; 45; 5; 1981; 1257-1260;

Isolation from Natural Product (14 of 30)

Isolation from Natural Product	Ulocladium sp.
Citation Pointer	5864041; Journal; Dahiya, Jagroop S.; Woods, Donald L.; Tewari, Jalpa P.; PYTCAS; Phytochemistry; EN; 27; 7; 1988; 2366;

Isolation from Natural Product (15 of 30)

Isolation from Natural Product	fruits of Javanese long pepper, Piper retrofractum Vahl.
Citation Pointer	5846053; Journal; Kikuzaki, Hiroe; Kawabata, Marona; Ishida, Etsuko; Akazawa, Yoko; Takei, Yoko; et al.; BBBIEJ; Biosci.Biotechnol.Biochem.; EN; 57; 8; 1993; 1329-1333;

Isolation from Natural Product (16 of 30)

Isolation from Natural Product	Anethum sowa (seeds)
Citation Pointer	5749938; Journal; Jain, A. K.; Sharma, N. D.; Gupta, S. R.; IJSBDB; Indian J.Chem.Sect.B; EN; 25; 1986; 979;

Isolation from Natural Product (17 of 30)

Isolation from Natural Product	pepper, fruits of Piper nigrum L.
Citation Pointer	5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Isolation from Natural Product (18 of 30)

Isolation from Natural Product	Piper retrofractum (Piperaceae)
Citation Pointer	5710925; Journal; Ahn, Jong-Woong; Ahn, Mi-Ja; Zee, Ok-Pyo; Kim, Eun-Joo; Lee, Sueg-Geun; et al.; PYTCAS; Phytochemistry; EN; 31; 10; 1992; 3609-3612;

Isolation from Natural Product (19 of 30)

Isolation from Natural Product	fruits of Piper longum L.
Citation Pointer	5673694; Journal; Tabuneng, Wnanbyr; Bando, Hideo; Amiya, Takashi; CPBTAL; Chem.Pharm.Bull.; EN; 31; 10; 1983; 3562-3565;

Isolation from Natural Product (20 of 30)

Isolation from Natural Product	Piper argyrophyllum Miq.
Citation Pointer	5575872; Journal; Banerji, Avijit; Nandi, Gopa; IJSBDB; Indian J.Chem.Sect.B; EN; 27; 1-12; 1988; 163-165;

Isolation from Natural Product (21 of 30)

Isolation from Natural Product	Piper nigrum L.
Citation Pointer	5510783; Journal; Das, B. P.; Jamal, Molla Yousuf; Choudhury, B.; JICSAH; J.Indian Chem.Soc.; EN; 67; 1; 1990; 72-73;

Isolation from Natural Product (22 of 30)

Isolation from Natural Product	Vork. u. Isol. aus Piper peepuloides
Citation Pointer	3143698; Journal; Dhar; Raina; PLMEAA; Planta Med.; 23; 1973; 295,296;

Isolation from Natural Product (23 of 30)

Isolation from Natural Product	aus schwarzem Pfeffer
Citation Pointer	3141492; Journal; Lurik et al.; PCJOAU; Pharm.Chem.J.(Engl.Transl.); 5; 8; 1971; 462; KHFZAN; Khim.Farm.Zh.; 5; 8; 1971; 15;

Isolation from Natural Product (24 of 30)

Isolation from Natural Product	aus Papaver aurantiacum
Citation Pointer	3132150; Journal; Madhusudhana et al.; CUSCAM; Curr.Sci.; 43; 1974; 76;

Isolation from Natural Product (25 of 30)

Isolation from Natural Product	aus Fruechten von Piper guineense
Citation Pointer	156361; Journal; Okogun,J.I.; Ekong,D.E.U.; JCPRB4; J.Chem.Soc.Perkin Trans.1; EN; 1974; 2195-2198;

Isolation from Natural Product (26 of 30)

Isolation from Natural Product	Findet sich in den unreifen Fruechten ('schwarzer Pfeffer') und in den Kernen der reifen Fruechte ('weisser Pfeffer') von Piper nigrum
Comment	Handbook
Citation Pointer	960850; Journal; Varrentrapp; Will; JLACBF; Justus Liebigs Ann. Chem.; 39; 1841; 283;960851; Journal; Regnault; ANCPAC; Ann.Chim.(Paris); <2> 68; 1838; 158;960852; Journal; Liebig; JLACBF; Justus Liebigs Ann. Chem.; 6; 1833; 36;960853; Journal; Pelletier; ANCPAC; Ann.Chim.(Paris); <2> 51; 1832; 199; JLACBF; Justus Liebigs Ann. Chem.; 6; 1833; 33;960854; Journal; Pelletier; ANCPAC; Ann.Chim.(Paris); <2> 16; 1821; 344; Schw.; 32; 436;960855; Journal; Oerstedt; Schweiggers Journ. f. Chemie u. Physik; 29; 80;

Isolation from Natural Product (27 of 30)

Isolation from Natural Product	Findet sich ferner im langen Pfeffer (reife Fruechte von P. longum und P. officinarum)
Comment	Handbook
Citation Pointer	960848; Journal; Wangerin; Pharm. Ztg.; 48; 454;960849; Journal; Bauer; Hilger; CHZEA6; Chem.Zentralbl.; GE; 67; I; 1896; 1214;

Isolation from Natural Product (28 of 30)

Isolation from Natural Product	in den Fruechten von P. Clusii (Aschantipfeffer)
Comment	Handbook
Citation Pointer	960846; Journal; Herlant; PHJOAV; Pharm.J.; <3> 25; 643;960847; Journal; Stenhouse; PHJOAV; Pharm.J.; <1> 14; 363; JLACBF; Justus Liebigs Ann. Chem.; 95; 1855; 106;

Isolation from Natural Product (29 of 30)

Isolation from Natural Product	in der Wurzelrinde von Artanthe geniculata (unechte Jaborandi)
Comment	Handbook
Citation Pointer	960845; Journal; Peckolt; Apoth. Ztg.; 10; 471;

Isolation from Natural Product (30 of 30)

Isolation from Natural Product	in den Fruechten von P. Lowong
Comment	Handbook
Citation Pointer	502948; Journal; Peinemann; ARPMAS; Arch.Pharm.(Weinheim Ger.); 234; 1896; 258;

Derivative (1 of 1)

Derivative BRN	288703
Derivative	1-(5-benzo[1,3]dioxol-5-yl-pentanoyl)-piperidine
Citation Pointer	5749938; Journal; Jain, A. K.; Sharma, N. D.; Gupta, S. R.; IJSBDB; Indian J.Chem.Sect.B; EN; 25; 1986; 979;

Related Structure (1 of 1)

Citation Pointer

3635101; Journal; De Cleyn; Verzele; BSCBAG; Bull.Soc.Chim.Belg.; 84; 1975; 435,436;

Crossfile Reference (1 of 4)

Name	Piperine, purum
Crossfile Source	Fluka
External Access ID	80810

Crossfile Reference (2 of 4)

Name	Piperidine, 1-<5-(1,3-benzodioxol-5-yl)-1-oxo-2,4-pentadienyl>-, (E,E)-
Crossfile Source	CRC Handbook of Chemistry and Physics
External Access ID	20134

Crossfile Reference (3 of 4)

Data Type	13C-NMR Spectrum
Crossfile Source	CSEARCH
External Access ID	SADT-12317

Crossfile Reference (4 of 4)

Data Type	13C-NMR Spectrum
Crossfile Source	CSEARCH
External Access ID	UNIW-14585

Crystal Property Description (1 of 2)

Colour & Other Properties	light-yellow
Citation Pointer	6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 - 2397;

Crystal Property Description (2 of 2)

Colour & Other Properties	Prismen
Comment	Handbook
Citation Pointer	967610; Journal; Tunmann; CHZEA6; Chem.Zentralbl.; GE; 89; II; 1918; 675;

Melting Point (1 of 19)

Solvent	ethyl acetate
Comment	Handbook
Citation Pointer	967610; Journal; Tunmann; CHZEA6; Chem.Zentralbl.; GE; 89; II; 1918; 675;

Melting Point (2 of 19)

Melting Point	131
Solvent	diethyl ether
Citation Pointer	5749938; Journal; Jain, A. K.; Sharma, N. D.; Gupta, S. R.; IJSBDB; Indian J.Chem.Sect.B; EN; 25; 1986; 979;

Melting Point (3 of 19)

Melting Point	132
Solvent	benzene
Citation Pointer	3132150; Journal; Madhusudhana et al.; CUSCAM; Curr.Sci.; 43; 1974; 76;

Melting Point (4 of 19)

Melting Point	130
Citation Pointer	5575872; Journal; Banerji, Avijit; Nandi, Gopa; IJSBDB; Indian J.Chem.Sect.B; EN; 27; 1-12; 1988; 163-165;

Melting Point (5 of 19)

Melting Point	130
Citation Pointer	3143698; Journal; Dhar; Raina; PLMEAA; Planta Med.; 23; 1973; 295,296;

Melting Point (6 of 19)

Melting Point	129.5
Comment	Handbook
Citation Pointer	502948; Journal; Peinemann; ARPMAS; Arch.Pharm.(Weinheim Ger.); 234; 1896; 258;

Melting Point (7 of 19)

Melting Point	129.5
Comment	Handbook
Citation Pointer	981397; Journal; Kofler,L.u.A.; Thermo-Mikro-Methoden,3.Aufl.; <Weinheim 1954> S.471;

Melting Point (8 of 19)

Melting Point	127
Citation Pointer	5975360; Journal; Dehmlow, Eckehard V.; Shamout, Abdul Rahman; JRMPDM; J.Chem.Res.Miniprint; GE; 4; 1981; 1178-1184;

Melting Point (9 of 19)

Melting Point	129
Citation Pointer	5874394; Journal; Nakatani, Nobuji; Inatani, Reiko; ABCHA6; Agric.Biol.Chem.; EN; 45; 6; 1981; 1473-1476;

Melting Point (10 of 19)

Melting Point	128
Citation Pointer	5576619; Journal; Banerji, Avijit; Ghosal, Tapasree; Acharyya, Aditi K.; IJSBDB; Indian J.Chem.Sect.B; EN; 23; 6; 1984; 546-549;

Melting Point (11 of 19)

Melting Point	129
Citation Pointer	3143025; Journal; Patra; Gosh; PYTCAS; Phytochemistry; 13; 1974; 2889;3635101; Journal; De Cleyn; Verzele; BSCBAG; Bull.Soc.Chim.Belg.; 84; 1975; 435,436;

Melting Point (12 of 19)

Melting Point	128
Citation Pointer	3140982; Journal; Grewe et al.; CHBEAM; Chem.Ber.; 103; 1970; 3752,3766;

Melting Point (13 of 19)

Melting Point	128.5 - 130
Citation Pointer	3714671; Journal; Meerov; Katyuzhanskaya; CHNCA8; Chem.Nat.Compd.(Engl.Transl.); 9; 1973; 179; KPSUAR; Khim.Prir.Soedin.; 9; 1973; 184;

Melting Point (14 of 19)

Melting Point	129 - 130
Citation Pointer	2995721; Patent; Haarmann and Reimer; DE 2757506; 1977;

Melting Point (15 of 19)

Melting Point	128 - 129.5
Citation Pointer	3141492; Journal; Lurik et al.; PCJOAU; Pharm.Chem.J.(Engl.Transl.); 5; 8; 1971; 462; KHFZAN; Khim.Farm.Zh.; 5; 8; 1971; 15;

Melting Point (16 of 19)

Melting Point	128 - 130
Citation Pointer	156361; Journal; Okogun,J.I.; Ekong,D.E.U.; JCPRB4; J.Chem.Soc.Perkin Trans.1; EN; 1974; 2195-2198;

Melting Point (17 of 19)

Melting Point	128 - 129.5
Comment	Handbook
Citation Pointer	960844; Journal; Ruegheimer; CHBEAM; Chem.Ber.; 15; 1882; 1391;

Melting Point (18 of 19)

Melting Point	128 - 129
Citation Pointer	6070238; Journal; Siddiqui, Bina S.; Begum, Sabira; Gulzar, Tahsin; Noor, Farhat and Fatima; PYTCAS; Phytochemistry; EN; 45; 8; 1997; 1617-1620;

Melting Point (19 of 19)

Melting Point	124
Citation Pointer	6205590; Journal; Pande, Archana; Shukla, Y. N.; Srivastava, Ritu; Verma, Monika; IJSBDB; Indian J.Chem.Sect.B; EN; 36; 4; 1997; 377 - 379;

Crystal Phase (1 of 8)

Description	Rate of crystallization
Comment	von unterkuehltem Piperin bei verschiedenen Temperaturen.; Handbook
Citation Pointer	969754; Journal; Tammann; ZEPCAC; Z.Phys.Chem.Stoechiom.Verwandtschaftsl.; 25; 1894; 450; ZAACAB; Z.Anorg.Allg.Chem.; 181; 1929; 413;

Crystal Phase (2 of 8)

Description	Rate of crystallization
Comment	von unterkuehltem Piperidin bei Drucken bis 1000 kg/cm2.; Handbook
Citation Pointer	969753; Journal; Hasselblatt; ZAACAB; Z.Anorg.Allg.Chem.; 119; 1921; 361;

Crystal Phase (3 of 8)

Description	Rate of crystallization
Comment	Geschwindigkeit der Bildung von Keimen bei der Kristallisation von unterkuehlten Schmelzen bei 20grad bzw. bei 48grad:.; Handbook
Citation Pointer	981393; Journal; Kondoguri; ZETFA7; Zh.Eksp.Teor.Fiz.; 11; 1941; 728; Chem.Abstr.; 1943; 1314;2200674; Journal; Michnewitsch; KOZHAG; Kolloidn.Zh.; 21; 1959; 69; engl. Ausg. S. 61;

Crystal Phase (4 of 8)

Description	Rate of crystallization
Comment	Keimbildung bei der Kristallisation von unterkuehlten Schmelzen in Abhaengigkeit von der Temperatur (72-80grad):.; Handbook
Citation Pointer	2175033; Journal; Tammann; Elsner v. Gronow; ZAACAB; Z.Anorg.Allg.Chem.; 200; 1931; 57, 68;

Crystal Phase (5 of 8)

Description	Rate of crystallization
Comment	in Abhaengigkeit von der Temperatur(0gradbis 90grad) und vom Reinheitsgrad:.; Handbook
Citation Pointer	981393; Journal; Kondoguri; ZETFA7; Zh.Eksp.Teor.Fiz.; 11; 1941; 728; Chem.Abstr.; 1943; 1314;

Crystal Phase (6 of 8)

Description	Rate of crystallization
Comment	Verstaerkte Keimbildung bei der Kristallisation von unterkuehlten Schmelzen bei Einwirkung von Ultraschall.; Handbook
Citation Pointer	2175021; Journal; Danilow; Tewerowskii; ZETFA7; Zh.Eksp.Teor.Fiz.; 10; 1940; 1305, 1308; Chem.Abstr.; 1941; 5368;

Crystal Phase (7 of 8)

Description	Interplanar spacing
Comment	von kristallinem und von fluessigem Piperin:.; Handbook
Citation Pointer	981396; Journal; Lewaschewitsch et al.; Trudy Dnetropetrovsk.chim.-technol.Inst.; 4; 1955; 84,88; Chem.Abstr.; 1959; 9760;

Crystal Phase (8 of 8)

Description	Solid state structure properties
Citation Pointer	3132105; Journal; Grynpas; Lindley; ACBCAR; Acta Crystallogr.Sect.B; 31; 1975; 2663,2664,2665,2666;

Sublimation (1 of 1)

Sublimation	104
Pressure	0.02
Comment	Handbook
Citation Pointer	636409; Journal; Janot; Chaigneau; COREAF; C.R.Hebd.Seances Acad.Sci.; 225; 1947; 1371;

Density of the Liquid (1 of 4)

Density of the Liquid	1.25
Comment	g/cm**3
Citation Pointer	3132105; Journal; Grynpas; Lindley; ACBCAR; Acta Crystallogr.Sect.B; 31; 1975; 2663,2664,2665,2666;

Density of the Liquid (2 of 4)

Density of the Liquid	1.192
Reference Temperature	4
Measurement Temperature	20
Comment	Handbook
Citation Pointer	981390; Journal; Kordes; ZPCBAL; Z.Phys.Chem.Abt.B; 43; 1939; 173,186;

Density of the Liquid (3 of 4)

Density of the Liquid	1.13
Measurement Temperature	113
Comment	g/cm**3; Handbook
Citation Pointer	969752; Journal; Tammann; Tampke; ZAACAB; Z.Anorg.Allg.Chem.; 162; 1927; 10;

Density of the Liquid (4 of 4)

Density of the Liquid	1.12
Measurement Temperature	136
Comment	g/cm**3; Handbook
Citation Pointer	969752; Journal; Tammann; Tampke; ZAACAB; Z.Anorg.Allg.Chem.; 162; 1927; 10;

Dynamic Viscosity (1 of 1)

Dynamic Viscosity	11.3
Temperature	95
Comment	Handbook
Citation Pointer	969749; Journal; Tammann; ZAACAB; Z.Anorg.Allg.Chem.; 181; 1929; 413;969752; Journal; Tammann; Tampke; ZAACAB; Z.Anorg.Allg.Chem.; 162; 1927; 10;969751; Journal; Tammann; Hesse; ZAACAB; Z.Anorg.Allg.Chem.; 156; 1926; 252;

Refractive Index (1 of 1)

Refractive Index	1.6846
Wavelength	589
Temperature	20
Comment	Handbook
Citation Pointer	981390; Journal; Kordes; ZPCBAL; Z.Phys.Chem.Abt.B; 43; 1939; 173,186;

Nuclear Magnetic Resonance (1 of 15)

Coupling Nuclei	1H-1H
Solvents	CDCl3
Frequency	500
Citation Pointer	6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 - 2397;

Nuclear Magnetic Resonance (2 of 15)

Description	Spectrum
Nucleus	1H
Temperature	41.9
Citation Pointer	5945187; Journal; Braumann, Urich; Haendel, heidrun; Albert, Klaus; Ecker, Rainer; Spraul, Manfred; ANCHAM; Anal.Chem.; EN; 67; 5; 1995; 930-935;

Nuclear Magnetic Resonance (3 of 15)

Description	Chemical shifts
Nucleus	13C
Solvents	CDCl3
Frequency	125.7
Citation Pointer	6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 - 2397;

Nuclear Magnetic Resonance (4 of 15)

Description	Chemical shifts
Nucleus	1H
Solvents	CDCl3
Frequency	500
Citation Pointer	6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 - 2397;

Nuclear Magnetic Resonance (5 of 15)

Description	Chemical shifts
Nucleus	1H
Solvents	CDCl3
Citation Pointer	6090513; Journal; Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain; SYNCAV; Synth.Commun.; EN; 28; 2; 1998; 239-250;

Nuclear Magnetic Resonance (6 of 15)

Description	Chemical shifts
Nucleus	13C
Solvents	CDCl3
Citation Pointer	6090513; Journal; Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain; SYNCAV; Synth.Commun.; EN; 28; 2; 1998; 239-250;

Nuclear Magnetic Resonance (7 of 15)

Description	Chemical shifts
Nucleus	1H
Solvents	CDCl3
Citation Pointer	5864041; Journal; Dahiya, Jagroop S.; Woods, Donald L.; Tewari, Jalpa P.; PYTCAS; Phytochemistry; EN; 27; 7; 1988; 2366;

Nuclear Magnetic Resonance (8 of 15)

Description	Chemical shifts
Nucleus	13C
Solvents	CDCl3
Citation Pointer	5787666; Journal; Banerji, Avijit; Sarkar, Manjusha (nee Chaudhuri); Ghosal, Tapasree; Pal, Sudhir Chandra; ORMRBD; Org.Magn.Reson.; EN; 22; 11; 1984; 734-736;

Nuclear Magnetic Resonance (9 of 15)

Description	Chemical shifts
Nucleus	1H
Solvents	CDCl3
Citation Pointer	5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Nuclear Magnetic Resonance (10 of 15)

Description	Chemical shifts
Nucleus	13C
Solvents	CDCl3
Citation Pointer	5576619; Journal; Banerji, Avijit; Ghosal, Tapasree; Acharyya, Aditi K.; IJSBDB; Indian J.Chem.Sect.B; EN; 23; 6; 1984; 546-549;5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Nuclear Magnetic Resonance (11 of 15)

Description	2D-NMR
Citation Pointer	5945187; Journal; Braumann, Urich; Haendel, heidrun; Albert, Klaus; Ecker, Rainer; Spraul, Manfred; ANCHAM; Anal.Chem.; EN; 67; 5; 1995; 930-935;

Nuclear Magnetic Resonance (12 of 15)

Description	NMR
Citation Pointer	3143025; Journal; Patra; Gosh; PYTCAS; Phytochemistry; 13; 1974; 2889;3633754; Journal; Wenkert et al.; JACSAT; J.Amer.Chem.Soc.; 93; 1971; 6271;3635101; Journal; De Cleyn; Verzele; BSCBAG; Bull.Soc.Chim.Belg.; 84; 1975; 435,436;

Nuclear Magnetic Resonance (13 of 15)

Description	Spin-spin coupling constants
Solvents	CDCl3
Comment	1H-1H
Citation Pointer	5864041; Journal; Dahiya, Jagroop S.; Woods, Donald L.; Tewari, Jalpa P.; PYTCAS; Phytochemistry; EN; 27; 7; 1988; 2366;6090513; Journal; Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain; SYNCAV; Synth.Commun.; EN; 28; 2; 1998; 239-250;

Nuclear Magnetic Resonance (14 of 15)

Description	Spin-spin coupling constants
Solvents	CDCl3
Comment	1H-13C.
Citation Pointer	5787666; Journal; Banerji, Avijit; Sarkar, Manjusha (nee Chaudhuri); Ghosal, Tapasree; Pal, Sudhir Chandra; ORMRBD; Org.Magn.Reson.; EN; 22; 11; 1984; 734-736;

Nuclear Magnetic Resonance (15 of 15)

Description	Spin-spin coupling constants
Solvents	CDCl3
Comment	1H-1H
Citation Pointer	5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Infrared Spectra (1 of 12)

Description	Bands
Solvent	KBr
Citation Pointer	6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 - 2397;

Infrared Spectra (2 of 12)

Description	Bands
Comment	3058 - 1043 cm**(-1)
Citation Pointer	6090513; Journal; Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain; SYNCAV; Synth.Commun.; EN; 28; 2; 1998; 239-250;

Infrared Spectra (3 of 12)

Description	Bands
Comment	1650 - 930 cm**(-1)
Citation Pointer	5864041; Journal; Dahiya, Jagroop S.; Woods, Donald L.; Tewari, Jalpa P.; PYTCAS; Phytochemistry; EN; 27; 7; 1988; 2366;

Infrared Spectra (4 of 12)

Description	Bands
Solvent	KBr
Comment	1635 - 925 cm**(-1)
Citation Pointer	5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Infrared Spectra (5 of 12)

Description	Bands
Solvent	CHCl3
Comment	1635 - 1585 cm**(-1)
Citation Pointer	5725528; Journal; Nakamura, Norio; Kiuchi, Fumiyuki; Tsuda, Yoshisuke; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2647-2651;

Infrared Spectra (6 of 12)

Description	Bands
Solvent	KBr
Comment	1635 - 1585 cm**(-1)
Citation Pointer	5725528; Journal; Nakamura, Norio; Kiuchi, Fumiyuki; Tsuda, Yoshisuke; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2647-2651;

Infrared Spectra (7 of 12)

Description	Bands
Solvent	KBr
Comment	1641 - 1624 cm**(-1)
Citation Pointer	5571390; Journal; Cabre, Juan; Palomo, Antonio Luis; SYNTBF; Synthesis; EN; 5; 1984; 413-417;

Infrared Spectra (8 of 12)

Description	Bands
Solvent	nujol
Comment	1600 - 780 cm**(-1); Handbook
Citation Pointer	642911; Journal; Pleat et al.; JPHAA3; J.Am.Pharm.Assoc.; 40; 1951; 107, 108;

Infrared Spectra (9 of 12)

Description	Bands
Solvent	KBr
Comment	3020 - 710 cm**(-1); Handbook
Citation Pointer	511899; Journal; Briggs et al.; ANCHAM; Anal.Chem.; 29; 1957; 904, 905;

Infrared Spectra (10 of 12)

Description	Bands
Solvent	CHCl3
Comment	1635 - 1580 cm**(-1); Handbook
Citation Pointer	511899; Journal; Briggs et al.; ANCHAM; Anal.Chem.; 29; 1957; 904, 905;1056240; Journal; Marion et al.; JACSAT; J.Amer.Chem.Soc.; 73; 1951; 305,; JACSAT; J.Amer.Chem.Soc.; 74; 1952; 270;

Infrared Spectra (11 of 12)

Description	Bands
Solvent	CHCl3
Comment	1490 - 930 cm**(-1); Handbook
Citation Pointer	511899; Journal; Briggs et al.; ANCHAM; Anal.Chem.; 29; 1957; 904, 905;1056240; Journal; Marion et al.; JACSAT; J.Amer.Chem.Soc.; 73; 1951; 305,; JACSAT; J.Amer.Chem.Soc.; 74; 1952; 270;

Infrared Spectra (12 of 12)

Description	IR
Citation Pointer	3132150; Journal; Madhusudhana et al.; CUSCAM; Curr.Sci.; 43; 1974; 76;3143025; Journal; Patra; Gosh; PYTCAS; Phytochemistry; 13; 1974; 2889;

Ultraviolet Spectra (1 of 10)

Description	Spectrum
Solvent	CHCl3
Comment	300 - 400 nm; Handbook
Citation Pointer	981386; Journal; Tausig et al.; JFOTAP; J.Food Technol.; 10; 1956; 151;

Ultraviolet Spectra (2 of 10)

Description	Spectrum
Solvent	ethanol
Comment	290 - 380 nm; Handbook
Citation Pointer	529237; Journal; Spring; Stark; JCSOA9; J.Chem.Soc.; 1950; 1177, 1178;